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edx  (JEOL)


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    JEOL edx
    ( A ) Binary phase map, showing the solubility of NaCTFSI/NaFSI at RT and crystallization behavior at −20°C. Soluble compositions at RT are shown in sky blue, whereas frozen compositions at −20°C are denoted by the capital letter “F.” The hybrid solution at α = 8 and β = 9 is the <t>only</t> <t>composition</t> that remained unfrozen (marked “N” in red). Inset photographs illustrate the crystallization behavior over time (1 to 48 hours) for representative compositions stored at −20°C. h, hours. ( B ) DSC curves of the hybrid solution during repeated heating and cooling cycles between −40° and 60°C at 1°C min −1 . ( C ) OCP variation over time on SS electrodes in 35 m NaFSI, 17.6 m NaCTFSI, and hybrid electrolytes. Inset photos show color differences of a methyl red indicator. ( D ) Potentiodynamic polarization curves on SS electrodes and corresponding FESEM images of SS surfaces after anodic polarization in the respective electrolytes. Scan rate = 1 mV s −1 . ( E ) EIS spectra at various temperatures and the corresponding Arrhenius plot (inset) in the 45.6 m hybrid electrolyte. ( F ) LSV curves of the 45.6 m hybrid electrolyte on SS and Al electrodes at 0.2 mV s −1 (cutoff current = ±10 μA cm −2 ). ( G ) Atomic compositions relative to Al, determined by <t>EDX</t> analysis of Al surfaces subjected to various negative potentials. Abnormally high “O” and “C” contents, arising from the surface oxide layer (Al 2 O 3 ) and surface-adsorbed CO 2 , are excluded.
    Edx, supplied by JEOL, used in various techniques. Bioz Stars score: 96/100, based on 1801 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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    edx - by Bioz Stars, 2026-06
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    1) Product Images from "A 45.6 m NaCTFSI/NaFSI hybrid electrolyte for high-voltage aqueous sodium-ion batteries operable at subzero temperatures"

    Article Title: A 45.6 m NaCTFSI/NaFSI hybrid electrolyte for high-voltage aqueous sodium-ion batteries operable at subzero temperatures

    Journal: Science Advances

    doi: 10.1126/sciadv.aef0138

    ( A ) Binary phase map, showing the solubility of NaCTFSI/NaFSI at RT and crystallization behavior at −20°C. Soluble compositions at RT are shown in sky blue, whereas frozen compositions at −20°C are denoted by the capital letter “F.” The hybrid solution at α = 8 and β = 9 is the only composition that remained unfrozen (marked “N” in red). Inset photographs illustrate the crystallization behavior over time (1 to 48 hours) for representative compositions stored at −20°C. h, hours. ( B ) DSC curves of the hybrid solution during repeated heating and cooling cycles between −40° and 60°C at 1°C min −1 . ( C ) OCP variation over time on SS electrodes in 35 m NaFSI, 17.6 m NaCTFSI, and hybrid electrolytes. Inset photos show color differences of a methyl red indicator. ( D ) Potentiodynamic polarization curves on SS electrodes and corresponding FESEM images of SS surfaces after anodic polarization in the respective electrolytes. Scan rate = 1 mV s −1 . ( E ) EIS spectra at various temperatures and the corresponding Arrhenius plot (inset) in the 45.6 m hybrid electrolyte. ( F ) LSV curves of the 45.6 m hybrid electrolyte on SS and Al electrodes at 0.2 mV s −1 (cutoff current = ±10 μA cm −2 ). ( G ) Atomic compositions relative to Al, determined by EDX analysis of Al surfaces subjected to various negative potentials. Abnormally high “O” and “C” contents, arising from the surface oxide layer (Al 2 O 3 ) and surface-adsorbed CO 2 , are excluded.
    Figure Legend Snippet: ( A ) Binary phase map, showing the solubility of NaCTFSI/NaFSI at RT and crystallization behavior at −20°C. Soluble compositions at RT are shown in sky blue, whereas frozen compositions at −20°C are denoted by the capital letter “F.” The hybrid solution at α = 8 and β = 9 is the only composition that remained unfrozen (marked “N” in red). Inset photographs illustrate the crystallization behavior over time (1 to 48 hours) for representative compositions stored at −20°C. h, hours. ( B ) DSC curves of the hybrid solution during repeated heating and cooling cycles between −40° and 60°C at 1°C min −1 . ( C ) OCP variation over time on SS electrodes in 35 m NaFSI, 17.6 m NaCTFSI, and hybrid electrolytes. Inset photos show color differences of a methyl red indicator. ( D ) Potentiodynamic polarization curves on SS electrodes and corresponding FESEM images of SS surfaces after anodic polarization in the respective electrolytes. Scan rate = 1 mV s −1 . ( E ) EIS spectra at various temperatures and the corresponding Arrhenius plot (inset) in the 45.6 m hybrid electrolyte. ( F ) LSV curves of the 45.6 m hybrid electrolyte on SS and Al electrodes at 0.2 mV s −1 (cutoff current = ±10 μA cm −2 ). ( G ) Atomic compositions relative to Al, determined by EDX analysis of Al surfaces subjected to various negative potentials. Abnormally high “O” and “C” contents, arising from the surface oxide layer (Al 2 O 3 ) and surface-adsorbed CO 2 , are excluded.

    Techniques Used: Solubility, Crystallization Assay



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    ( A ) Binary phase map, showing the solubility of NaCTFSI/NaFSI at RT and crystallization behavior at −20°C. Soluble compositions at RT are shown in sky blue, whereas frozen compositions at −20°C are denoted by the capital letter “F.” The hybrid solution at α = 8 and β = 9 is the <t>only</t> <t>composition</t> that remained unfrozen (marked “N” in red). Inset photographs illustrate the crystallization behavior over time (1 to 48 hours) for representative compositions stored at −20°C. h, hours. ( B ) DSC curves of the hybrid solution during repeated heating and cooling cycles between −40° and 60°C at 1°C min −1 . ( C ) OCP variation over time on SS electrodes in 35 m NaFSI, 17.6 m NaCTFSI, and hybrid electrolytes. Inset photos show color differences of a methyl red indicator. ( D ) Potentiodynamic polarization curves on SS electrodes and corresponding FESEM images of SS surfaces after anodic polarization in the respective electrolytes. Scan rate = 1 mV s −1 . ( E ) EIS spectra at various temperatures and the corresponding Arrhenius plot (inset) in the 45.6 m hybrid electrolyte. ( F ) LSV curves of the 45.6 m hybrid electrolyte on SS and Al electrodes at 0.2 mV s −1 (cutoff current = ±10 μA cm −2 ). ( G ) Atomic compositions relative to Al, determined by <t>EDX</t> analysis of Al surfaces subjected to various negative potentials. Abnormally high “O” and “C” contents, arising from the surface oxide layer (Al 2 O 3 ) and surface-adsorbed CO 2 , are excluded.
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    ( A ) Binary phase map, showing the solubility of NaCTFSI/NaFSI at RT and crystallization behavior at −20°C. Soluble compositions at RT are shown in sky blue, whereas frozen compositions at −20°C are denoted by the capital letter “F.” The hybrid solution at α = 8 and β = 9 is the <t>only</t> <t>composition</t> that remained unfrozen (marked “N” in red). Inset photographs illustrate the crystallization behavior over time (1 to 48 hours) for representative compositions stored at −20°C. h, hours. ( B ) DSC curves of the hybrid solution during repeated heating and cooling cycles between −40° and 60°C at 1°C min −1 . ( C ) OCP variation over time on SS electrodes in 35 m NaFSI, 17.6 m NaCTFSI, and hybrid electrolytes. Inset photos show color differences of a methyl red indicator. ( D ) Potentiodynamic polarization curves on SS electrodes and corresponding FESEM images of SS surfaces after anodic polarization in the respective electrolytes. Scan rate = 1 mV s −1 . ( E ) EIS spectra at various temperatures and the corresponding Arrhenius plot (inset) in the 45.6 m hybrid electrolyte. ( F ) LSV curves of the 45.6 m hybrid electrolyte on SS and Al electrodes at 0.2 mV s −1 (cutoff current = ±10 μA cm −2 ). ( G ) Atomic compositions relative to Al, determined by <t>EDX</t> analysis of Al surfaces subjected to various negative potentials. Abnormally high “O” and “C” contents, arising from the surface oxide layer (Al 2 O 3 ) and surface-adsorbed CO 2 , are excluded.
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    ( A ) Binary phase map, showing the solubility of NaCTFSI/NaFSI at RT and crystallization behavior at −20°C. Soluble compositions at RT are shown in sky blue, whereas frozen compositions at −20°C are denoted by the capital letter “F.” The hybrid solution at α = 8 and β = 9 is the <t>only</t> <t>composition</t> that remained unfrozen (marked “N” in red). Inset photographs illustrate the crystallization behavior over time (1 to 48 hours) for representative compositions stored at −20°C. h, hours. ( B ) DSC curves of the hybrid solution during repeated heating and cooling cycles between −40° and 60°C at 1°C min −1 . ( C ) OCP variation over time on SS electrodes in 35 m NaFSI, 17.6 m NaCTFSI, and hybrid electrolytes. Inset photos show color differences of a methyl red indicator. ( D ) Potentiodynamic polarization curves on SS electrodes and corresponding FESEM images of SS surfaces after anodic polarization in the respective electrolytes. Scan rate = 1 mV s −1 . ( E ) EIS spectra at various temperatures and the corresponding Arrhenius plot (inset) in the 45.6 m hybrid electrolyte. ( F ) LSV curves of the 45.6 m hybrid electrolyte on SS and Al electrodes at 0.2 mV s −1 (cutoff current = ±10 μA cm −2 ). ( G ) Atomic compositions relative to Al, determined by <t>EDX</t> analysis of Al surfaces subjected to various negative potentials. Abnormally high “O” and “C” contents, arising from the surface oxide layer (Al 2 O 3 ) and surface-adsorbed CO 2 , are excluded.
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    ( A ) Binary phase map, showing the solubility of NaCTFSI/NaFSI at RT and crystallization behavior at −20°C. Soluble compositions at RT are shown in sky blue, whereas frozen compositions at −20°C are denoted by the capital letter “F.” The hybrid solution at α = 8 and β = 9 is the <t>only</t> <t>composition</t> that remained unfrozen (marked “N” in red). Inset photographs illustrate the crystallization behavior over time (1 to 48 hours) for representative compositions stored at −20°C. h, hours. ( B ) DSC curves of the hybrid solution during repeated heating and cooling cycles between −40° and 60°C at 1°C min −1 . ( C ) OCP variation over time on SS electrodes in 35 m NaFSI, 17.6 m NaCTFSI, and hybrid electrolytes. Inset photos show color differences of a methyl red indicator. ( D ) Potentiodynamic polarization curves on SS electrodes and corresponding FESEM images of SS surfaces after anodic polarization in the respective electrolytes. Scan rate = 1 mV s −1 . ( E ) EIS spectra at various temperatures and the corresponding Arrhenius plot (inset) in the 45.6 m hybrid electrolyte. ( F ) LSV curves of the 45.6 m hybrid electrolyte on SS and Al electrodes at 0.2 mV s −1 (cutoff current = ±10 μA cm −2 ). ( G ) Atomic compositions relative to Al, determined by <t>EDX</t> analysis of Al surfaces subjected to various negative potentials. Abnormally high “O” and “C” contents, arising from the surface oxide layer (Al 2 O 3 ) and surface-adsorbed CO 2 , are excluded.
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    The schematic illustrates four interconnected components that together provide a comprehensive assessment of ITN performance. Bioassays are used to determine product bio-efficacy through standardized mosquito exposure protocols. Chemical analysis via HPLC and GC-MS enables quantification of AIs, identification of isomeric forms, and assessment of chemical stability. Surface imaging, using scanning electron <t>microscopy</t> <t>(SEM)/energy-dispersive</t> x-ray <t>(EDX)</t> and Raman spectroscopy, provides insight into the spatial distribution and molecular characteristics of insecticide deposition on net fibers. Video analysis technologies are used to monitor mosquito behavior during exposure, offering dynamic data on contact duration, avoidance, and sublethal responses. These components converge to define the chemical presentation of the insecticide and its bio-efficacy, forming a core metric for comparing ITN performance across products and resistance profiles.
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    Image Search Results


    ( A ) Binary phase map, showing the solubility of NaCTFSI/NaFSI at RT and crystallization behavior at −20°C. Soluble compositions at RT are shown in sky blue, whereas frozen compositions at −20°C are denoted by the capital letter “F.” The hybrid solution at α = 8 and β = 9 is the only composition that remained unfrozen (marked “N” in red). Inset photographs illustrate the crystallization behavior over time (1 to 48 hours) for representative compositions stored at −20°C. h, hours. ( B ) DSC curves of the hybrid solution during repeated heating and cooling cycles between −40° and 60°C at 1°C min −1 . ( C ) OCP variation over time on SS electrodes in 35 m NaFSI, 17.6 m NaCTFSI, and hybrid electrolytes. Inset photos show color differences of a methyl red indicator. ( D ) Potentiodynamic polarization curves on SS electrodes and corresponding FESEM images of SS surfaces after anodic polarization in the respective electrolytes. Scan rate = 1 mV s −1 . ( E ) EIS spectra at various temperatures and the corresponding Arrhenius plot (inset) in the 45.6 m hybrid electrolyte. ( F ) LSV curves of the 45.6 m hybrid electrolyte on SS and Al electrodes at 0.2 mV s −1 (cutoff current = ±10 μA cm −2 ). ( G ) Atomic compositions relative to Al, determined by EDX analysis of Al surfaces subjected to various negative potentials. Abnormally high “O” and “C” contents, arising from the surface oxide layer (Al 2 O 3 ) and surface-adsorbed CO 2 , are excluded.

    Journal: Science Advances

    Article Title: A 45.6 m NaCTFSI/NaFSI hybrid electrolyte for high-voltage aqueous sodium-ion batteries operable at subzero temperatures

    doi: 10.1126/sciadv.aef0138

    Figure Lengend Snippet: ( A ) Binary phase map, showing the solubility of NaCTFSI/NaFSI at RT and crystallization behavior at −20°C. Soluble compositions at RT are shown in sky blue, whereas frozen compositions at −20°C are denoted by the capital letter “F.” The hybrid solution at α = 8 and β = 9 is the only composition that remained unfrozen (marked “N” in red). Inset photographs illustrate the crystallization behavior over time (1 to 48 hours) for representative compositions stored at −20°C. h, hours. ( B ) DSC curves of the hybrid solution during repeated heating and cooling cycles between −40° and 60°C at 1°C min −1 . ( C ) OCP variation over time on SS electrodes in 35 m NaFSI, 17.6 m NaCTFSI, and hybrid electrolytes. Inset photos show color differences of a methyl red indicator. ( D ) Potentiodynamic polarization curves on SS electrodes and corresponding FESEM images of SS surfaces after anodic polarization in the respective electrolytes. Scan rate = 1 mV s −1 . ( E ) EIS spectra at various temperatures and the corresponding Arrhenius plot (inset) in the 45.6 m hybrid electrolyte. ( F ) LSV curves of the 45.6 m hybrid electrolyte on SS and Al electrodes at 0.2 mV s −1 (cutoff current = ±10 μA cm −2 ). ( G ) Atomic compositions relative to Al, determined by EDX analysis of Al surfaces subjected to various negative potentials. Abnormally high “O” and “C” contents, arising from the surface oxide layer (Al 2 O 3 ) and surface-adsorbed CO 2 , are excluded.

    Article Snippet: The elemental composition of the synthesized electrode materials was determined by EDX coupled with FESEM (JSM-7610F Plus, JEOL, Japan).

    Techniques: Solubility, Crystallization Assay

    The schematic illustrates four interconnected components that together provide a comprehensive assessment of ITN performance. Bioassays are used to determine product bio-efficacy through standardized mosquito exposure protocols. Chemical analysis via HPLC and GC-MS enables quantification of AIs, identification of isomeric forms, and assessment of chemical stability. Surface imaging, using scanning electron microscopy (SEM)/energy-dispersive x-ray (EDX) and Raman spectroscopy, provides insight into the spatial distribution and molecular characteristics of insecticide deposition on net fibers. Video analysis technologies are used to monitor mosquito behavior during exposure, offering dynamic data on contact duration, avoidance, and sublethal responses. These components converge to define the chemical presentation of the insecticide and its bio-efficacy, forming a core metric for comparing ITN performance across products and resistance profiles.

    Journal: Science Advances

    Article Title: Multimodal platform for ITN efficacy: Surface chemistry, bioavailability, and mosquito behavior

    doi: 10.1126/sciadv.aeb2023

    Figure Lengend Snippet: The schematic illustrates four interconnected components that together provide a comprehensive assessment of ITN performance. Bioassays are used to determine product bio-efficacy through standardized mosquito exposure protocols. Chemical analysis via HPLC and GC-MS enables quantification of AIs, identification of isomeric forms, and assessment of chemical stability. Surface imaging, using scanning electron microscopy (SEM)/energy-dispersive x-ray (EDX) and Raman spectroscopy, provides insight into the spatial distribution and molecular characteristics of insecticide deposition on net fibers. Video analysis technologies are used to monitor mosquito behavior during exposure, offering dynamic data on contact duration, avoidance, and sublethal responses. These components converge to define the chemical presentation of the insecticide and its bio-efficacy, forming a core metric for comparing ITN performance across products and resistance profiles.

    Article Snippet: All SEM images and EDX spectra were acquired using a JEOL JSM 7001F SEM System with using the Oxford Instruments INCA software for SEM images acquisitions.

    Techniques: Gas Chromatography-Mass Spectrometry, Imaging, Electron Microscopy, Raman Spectroscopy

    ( A ) Top row, PFAS (+) net: SEM images at ×500 magnification from two example areas on the PFAS (+) net surface. Area 1 represents the same PFAS (+) area shown in at ×500 magnification. Corresponding EDX spectra were obtained at specific particulate locations marked with crosses. The representative EDX spectrum from PFAS (+) net reveals the presence of bromine (Br), fluorine (F), and chlorine (Cl), confirming deltamethrin and specific PFAS formulation. ( B ) Bottom row, PFAS (−) net: SEM image at ×500 magnification from two example areas on the PFAS (−) net surface. Area 1 represents the same PFAS (−) sample area shown in at ×500 magnification. Corresponding EDX spectra were obtained at the locations marked with crosses. The representative EDX spectrum of PFAS (−) net shows the presence of bromine (Br) but no fluorine (F) or chlorine (Cl), indicating a change in the formulation used in 2019. cps, counts per second.

    Journal: Science Advances

    Article Title: Multimodal platform for ITN efficacy: Surface chemistry, bioavailability, and mosquito behavior

    doi: 10.1126/sciadv.aeb2023

    Figure Lengend Snippet: ( A ) Top row, PFAS (+) net: SEM images at ×500 magnification from two example areas on the PFAS (+) net surface. Area 1 represents the same PFAS (+) area shown in at ×500 magnification. Corresponding EDX spectra were obtained at specific particulate locations marked with crosses. The representative EDX spectrum from PFAS (+) net reveals the presence of bromine (Br), fluorine (F), and chlorine (Cl), confirming deltamethrin and specific PFAS formulation. ( B ) Bottom row, PFAS (−) net: SEM image at ×500 magnification from two example areas on the PFAS (−) net surface. Area 1 represents the same PFAS (−) sample area shown in at ×500 magnification. Corresponding EDX spectra were obtained at the locations marked with crosses. The representative EDX spectrum of PFAS (−) net shows the presence of bromine (Br) but no fluorine (F) or chlorine (Cl), indicating a change in the formulation used in 2019. cps, counts per second.

    Article Snippet: All SEM images and EDX spectra were acquired using a JEOL JSM 7001F SEM System with using the Oxford Instruments INCA software for SEM images acquisitions.

    Techniques: Formulation